By K. P. Lawley
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Sinica (Peking) 14: 1710. , 1961, Amino acid chI oro phenyl esters. II. Synthesis of pep tides by aminolysis of active N-protected amino acid 2,4,6-trichlorophenyl esters, Roczniki Chern. 35: 595; Chern. Abst. 57:27121i, 1961. , 1963, Amino acid chlorophenyl esters. VII. Reaction of phthaloylglycine chlorophenyl esters with benzyl amine, Roczniki Chern. 37: 161; Chern. Abst. 59: 11651e, 1963. , Mat. Fiz. Chern. Wyzsza Szk. Pedagog. Gdansku 7: 159; Chern. Abst. 70:47839r, 1969. , 1968, The application of active Nacylated amino acid [N-(2-pyrimidyl)sulfonamido] phenyl esters for the synthesis of peptide bonds, Roczniki Chern.
1955, Ober aktivierte Ester. V. Verwendung der Cyanmethylester-Methode zur Herstellung von (N-Carbobenzoxy-S-benzyl-L-cysteinyl)L-tyrosyl-L-isoleucin auf verschiedenen Wegen, Helv. Chim. Acta 38: 1508. Jakubke, H. D .. 1965a. Darstellung N-geschtitzter Aminosiiureester des 8-Hydroxychinolins und deren Verwendung als reaktive Zwischenprodukte fUr die Peptidsynthese, Z. Naturforsch. 20b: 273. Jakubke, H. D .. 1965b. Ober aktivierte Ester; Peptidsynthese mit N-Acylaminosiiure-8thiochinolyl Estern.
1969). In principle, only the e-amino group of lysine and -SH groups of cysteine residues need to be protected. The difficulties encountered in the purification of longer chains carrying numerous protecting groups suggest that, in the synthesis oflarge molecules, minimal protection is to be preferred, and hence further application of active esters, both in solution and in SPPS, can be expected in the future. REFERENCES Anderson, G. W .. Zimmerman, J. , and Callahan, F. , 1963, N-Hydroxysuccinimide esters in peptide synthesis, J.